(n-Bu)2InSPh

Base Information

• Chemical Name: (n-Bu)2InSPh
• CAS No.: 123373-99-9
• Molecular Formula: C₁₄H₂₃InS
• Molecular Weight: 338.223
• Mol file: 123373-99-9.mol

Synonyms:

Chemical Property of (n-Bu)2InSPh

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (n-Bu)2InSPh

There total 1 articles about (n-Bu)2InSPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

tri-n-butylindium (15676-66-1) + thiophenol (108-98-5) → (n-Bu)2InSPh (123373-99-9)

Guidance literature:

In diethyl ether; dry N2-atmosphere, equimolar amts. of (n-Bu)3In/thiol, addn. of In-compd. dissolved in abs. ether to thiol dropwise at -78°C with stirring, warming up to room temperature and stirring (6 h); removing solvent and unreacted thiol in vac., recrystn. from (ether/hexane); elem. anal.;

DOI:10.1016/S0277-5387(00)83845-0

upstream raw materials:

tri-n-butylindium

thiophenol