Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin)

Base Information

• Chemical Name: Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin)
• CAS No.: 1228359-35-0
• Molecular Formula: C₅₈H₅₅GdN₄O₃
• Molecular Weight: 1013.35

Synonyms:

Chemical Property of Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin)

Chemical Property:

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Technology Process of Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin)

There total 1 articles about Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

gadolinium(III) chloride hexahydrate + 5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin → Gd(OH)(5-(4-myristyloxy)phenyl-10,15,20-triphenyl porphyrin) (1228359-35-0)

Guidance literature:

With imidazole; In further solvent(s); mixture of porphyrin-compd. and Gd-compd. heated in an imidazole melt at210°C under N2 for 2 h with stirring, cooled to 100°C; H2O added, filtered, washed with H2O, dried in vac., dissolved in CHCl3,shaken with 0.1% aq. AgNO3, CHCl3 layer searated, concentrated, chromy. (aluminium oxide, CHCl3-20%CH3OH), crystallized by concentrated, dried in vac., elem. anal.;

DOI:10.1080/15533170903328537

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