C₂₈H₂₉NO₅

Base Information

Chemical Name:C₂₈H₂₉NO₅
CAS No.:1415722-83-6
Molecular Formula:C₂₈H₂₉NO₅
Molecular Weight:459.542
Hs Code.:

C<sub>28</sub>H<sub>29</sub>NO<sub>5</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₉NO₅

Chemical Property:

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Technology Process of C₂₈H₂₉NO₅

There total 9 articles about C₂₈H₂₉NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1415684-46-6
C₂₈H₂₇NO₅

: 1415722-83-6,1415723-39-5
C₂₈H₂₉NO₅

Guidance literature:: With platinum on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 2.5h; under 760.051 Torr; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 1415722-83-6,1415723-39-5
C₂₈H₂₉NO₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 5 h / Reflux; Inert atmosphere

2.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

2.2: 15 h / 20 - 140 °C / Inert atmosphere

3.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 20 °C / Inert atmosphere

5.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

6.1: benzene / 1 h / 20 °C / Inert atmosphere

7.1: platinum on carbon; hydrogen / ethyl acetate / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

With chromium(VI) oxide; platinum on carbon; hydrogen; copper; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; Triethylene glycol dimethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 1415684-40-0
C₂₁H₁₇IO₃

: 1415722-83-6,1415723-39-5
C₂₈H₂₉NO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

1.2: 15 h / 20 - 140 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 19 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

5.1: benzene / 1 h / 20 °C / Inert atmosphere

6.1: platinum on carbon; hydrogen / ethyl acetate / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

With chromium(VI) oxide; platinum on carbon; hydrogen; copper; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; Triethylene glycol dimethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092