Technology Process of C54H63N10O7P
There total 11 articles about C54H63N10O7P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1h;
DOI:10.1093/nar/gkr010
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide / ethyl acetate / 14 h / 20 °C
2.1: pyridine / 2 h
3.1: 3 h
4.1: water / 0.25 h
4.2: 0.5 h
5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
With
pyridine; copper(l) iodide; water; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; ethyl acetate;
DOI:10.1093/nar/gkr010
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 40 °C
2.1: pyridine / 20 °C
3.1: ammonia / water / 12 h / 20 °C
4.1: copper(l) iodide / ethyl acetate / 14 h / 20 °C
5.1: pyridine / 2 h
6.1: 3 h
7.1: water / 0.25 h
7.2: 0.5 h
8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h
With
pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); ammonia; water; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate;
1.1: Sonogashira coupling;
DOI:10.1093/nar/gkr010