C₂₂H₁₅N₃O₅S

Base Information

• Chemical Name: C₂₂H₁₅N₃O₅S
• CAS No.: 1417334-76-9
• Molecular Formula: C₂₂H₁₅N₃O₅S
• Molecular Weight: 433.444
• Mol file: 1417334-76-9.mol

Synonyms:

Chemical Property of C₂₂H₁₅N₃O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₅N₃O₅S

There total 6 articles about C₂₂H₁₅N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3,4-methylenedioxybenzoate (326-56-7) → C22H15N3O5S (1417334-76-9)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 48 h / Reflux

2: triethylamine / ethanol / Inert atmosphere; Reflux

3: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C

With hydrazine hydrate; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.06.006

Reference yield:

Piperonylic acid (94-53-1) → C22H15N3O5S (1417334-76-9)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride / 13 h / 0 - 50 °C / Inert atmosphere

2: hydrazine hydrate / ethanol / 48 h / Reflux

3: triethylamine / ethanol / Inert atmosphere; Reflux

4: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C

With thionyl chloride; hydrazine hydrate; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.06.006

Reference yield:

benzo[d][1,3]dioxole-5-carbohydrazide (22026-39-7) → C22H15N3O5S (1417334-76-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethanol / Inert atmosphere; Reflux

2: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C

With triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.06.006

upstream raw materials:

methyl 3,4-methylenedioxybenzoate

Piperonylic acid

4-methyl-2'-nitrobiphenyl

benzo[d][1,3]dioxole-5-carbohydrazide