{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

Base Information

Chemical Name:{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol
CAS No.:151799-35-8
Molecular Formula:C₃₆H₄₇O₇P
Molecular Weight:622.739
Hs Code.:

{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

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Chemical Property of {3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

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Technology Process of {3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

There total 12 articles about {3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151799-40-5
C₄₈H₇₅O₇PSi₂

: 151799-35-8
{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

Guidance literature:: With tetrabutyl ammonium fluoride;

Reference yield:

: 41492-05-1
p-bromobutylbenzene

: 151799-35-8
{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Mg / 1.) THF, 2.) THF

2: LiAlH₄

3: n-BuLi

4: H₂O₂

5: n-Bu₄NF

With lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; dihydrogen peroxide; magnesium;

Reference yield:

: 89-32-7,34527-94-1
Pyromellitic dianhydride

: 151799-35-8
{3-[(4-Butyl-phenyl)-(3-hydroxymethyl-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-ylmethyl)-phosphinoylmethyl]-7,7-dimethyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-2-yl}-methanol

Guidance literature:: Multi-step reaction with 9 steps

1: H₂SO₄

2: LiAlH₄

3: p-TsOH

4: LiAlH₄

5: 1.) NaH

6: Et₃N

7: n-BuLi

8: H₂O₂

9: n-Bu₄NF

With lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hydride; toluene-4-sulfonic acid; triethylamine;