[Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)

Base Information

Chemical Name:[Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)
CAS No.:1310358-22-5
Molecular Formula:C₅₉H₅₂Cl₂N₄OP₃Pd₂S*NO₃
Molecular Weight:1303.83
Hs Code.:

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Suppliers and Price of [Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)

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Technology Process of [Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)

There total 1 articles about [Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 22278-76-8
4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one

: silver nitrate

: 603-35-0
triphenylphosphine

: palladium dichloride

: 1310358-22-5
[Pd2Cl2(triphenylphosphane)3(κ2N,S:κ1N-4-amino-6-ethyl-1,2,4-triazine-3-thion-5-one(-H))](nitrate)

Guidance literature:: With CH₃COONa; In methanol; acetonitrile; byproducts: NaCl, AgCl, CH3COOH; addn. of palladium compd. and phosphane deriv. to soln. of triazine deriv. and sodium acetate in methanol/CH3CN (1:1), stirring for 3 h, addn. of soln. of silver nitrate in CH3OH/CH3CN (1:1), stirring for 3 h; filtration, washing with cold methanol, keeping filtrate at 4°C for few wks, isolation of crystals, elem. anal.;
DOI:10.1016/j.poly.2011.03.048