C₁₆H₂₄OSi

Base Information Edit

Chemical Name:C₁₆H₂₄OSi
CAS No.:1310330-37-0
Molecular Formula:C₁₆H₂₄OSi
Molecular Weight:260.451
Hs Code.:
Mol file:1310330-37-0.mol

Synonyms:

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Chemical Property of C₁₆H₂₄OSi Edit

Chemical Property:

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Technology Process of C₁₆H₂₄OSi

There total 5 articles about C₁₆H₂₄OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: (Z)-5-(Benzyl-dimethyl-silanyl)-5-iodo-pent-4-en-1-ol

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1310330-37-0
C₁₆H₂₄OSi

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In N,N-dimethyl-formamide; for 1h; Inert atmosphere;
DOI:10.1021/ja2031085

Reference yield:

: 460752-64-1
5-(benzyldimethylsilyl)pent-4-yn-1-ol

: 1310330-37-0
C₁₆H₂₄OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylaluminum / dichloromethane; toluene / 0 - 20 °C / Inert atmosphere

1.2: 58 h / 20 °C / Inert atmosphere

1.3: 1 h / -78 - 0 °C / Inert atmosphere

2.1: dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 1 h / Inert atmosphere

With dichloro bis(acetonitrile) palladium(II); triethylaluminum; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja2031085

Reference yield:

: 259874-44-7
5-(benzyldimethylsilyl)-1-(tetrahydropyran-2′-yloxy)pent-4-yne

: 1310330-37-0
C₁₆H₂₄OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; toluene-4-sulfonic acid / 2 h / Inert atmosphere

2.1: triethylaluminum / dichloromethane; toluene / 0 - 20 °C / Inert atmosphere

2.2: 58 h / 20 °C / Inert atmosphere

2.3: 1 h / -78 - 0 °C / Inert atmosphere

3.1: dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 1 h / Inert atmosphere

With methanol; dichloro bis(acetonitrile) palladium(II); triethylaluminum; toluene-4-sulfonic acid; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja2031085