1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone

Base Information

• Chemical Name: 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone
• CAS No.: 22255-29-4
• Molecular Formula: C₂₁H₂₀O₁₀
• Molecular Weight: 432.384
• Mol file: 22255-29-4.mol

Synonyms:

Chemical Property of 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone

Chemical Property:

• Boiling Point: 778.9±60.0 °C(Predicted)
• Density: 1.673±0.06 g/cm3(Predicted)

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

Lucidin 3-O-glucoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone

There total 3 articles about 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

lucidin-3-primeveroside (29706-59-0,37393-11-6) → 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone (22255-29-4)

Guidance literature:

With hydrogenchloride; at 90 ℃; for 1.5h;

DOI:10.1016/S0031-9422(02)00095-X

Reference yield:

→ lucidin-3-O-β-glucoside (22255-29-4)

Guidance literature:

DOI:10.1007/BF00568525

Reference yield:

→ 1-Hydroxy-2-hydroxymethyl-3-((3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-anthraquinone (22255-29-4)

Guidance literature:

schrittweise Hydrolyse von Lucidin-primver?osid (IX);

DOI:10.1007/BF00633289

upstream raw materials:

lucidin-3-primeveroside

Downstream raw materials:

1,3-dihydroxy-2-hydroxymethyl-9,10-anthraquinone