ClH*C₂₂H₂₆N₂O₅

Base Information

Chemical Name:ClH*C₂₂H₂₆N₂O₅
CAS No.:1415334-02-9
Molecular Formula:C₂₂H₂₆N₂O₅*ClH
Molecular Weight:434.92
Hs Code.:

ClH*C<sub>22</sub>H<sub>26</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of ClH*C₂₂H₂₆N₂O₅

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Technology Process of ClH*C₂₂H₂₆N₂O₅

There total 4 articles about ClH*C₂₂H₂₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2380-94-1
1H-indol-4-ol

: 1415334-02-9
ClH*C₂₂H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine; dmap / dichloromethane / 20 °C

2: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C

3: trichlorophosphate / 0.75 h / 10 - 35 °C / Inert atmosphere

4: pyridine; piperidine / Reflux

5: palladium 10% on activated carbon; ammonium formate / ethanol / 1 h / Reflux

6: sodium cyanoborohydride; acetic acid / 20 °C

7: hydrogenchloride / methanol; water

With piperidine; pyridine; hydrogenchloride; dmap; palladium 10% on activated carbon; tetrabutylammomium bromide; ammonium formate; sodium cyanoborohydride; acetic acid; triethylamine; sodium hydroxide; trichlorophosphate; In methanol; ethanol; dichloromethane; water; 3: |Vilsmeier-Haack Formylation / 4: |Knoevenagel Condensation;
DOI:10.1021/jm301411g

Reference yield:

: 1415381-46-2
3-(2-(methoxycarbonyl)ethyl)-1-methylindolin-4-yl 4-methoxyphenyl(methyl)carbamate

: 1415334-02-9
ClH*C₂₂H₂₆N₂O₅

Guidance literature:: With hydrogenchloride; In methanol; water;
DOI:10.1021/jm301411g

Reference yield:

: 1415333-19-5
1H-indol-4-yl (4-methoxyphenyl)(methyl)carbamate

: 1415334-02-9
ClH*C₂₂H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C

2: trichlorophosphate / 0.75 h / 10 - 35 °C / Inert atmosphere

3: pyridine; piperidine / Reflux

4: palladium 10% on activated carbon; ammonium formate / ethanol / 1 h / Reflux

5: sodium cyanoborohydride; acetic acid / 20 °C

6: hydrogenchloride / methanol; water

With piperidine; pyridine; hydrogenchloride; palladium 10% on activated carbon; tetrabutylammomium bromide; ammonium formate; sodium cyanoborohydride; acetic acid; sodium hydroxide; trichlorophosphate; In methanol; ethanol; dichloromethane; water; 2: |Vilsmeier-Haack Formylation / 3: |Knoevenagel Condensation;
DOI:10.1021/jm301411g