C₂₆H₁₈Cl₃FN₂O₄S

Base Information

Chemical Name:C₂₆H₁₈Cl₃FN₂O₄S
CAS No.:1416326-47-0
Molecular Formula:C₂₆H₁₈Cl₃FN₂O₄S
Molecular Weight:579.863
Hs Code.:

C<sub>26</sub>H<sub>18</sub>Cl<sub>3</sub>FN<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₆H₁₈Cl₃FN₂O₄S

Chemical Property:

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Technology Process of C₂₆H₁₈Cl₃FN₂O₄S

There total 4 articles about C₂₆H₁₈Cl₃FN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15658-60-3
diethyl-2,6-pyridinedicarbonyl ester

: 1416326-47-0
C₂₆H₁₈Cl₃FN₂O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / ethanol

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane

3.1: ethylmagnesium bromide / dichloromethane

4.1: hydrogen; palladium on activated charcoal; zinc dibromide / ethyl acetate

5.1: potassium carbonate / ethanol

5.2: Reflux

6.1: acetic acid / toluene

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With sodium tetrahydroborate; palladium on activated charcoal; ethylmagnesium bromide; hydrogen; sulfur trioxide pyridine complex; potassium carbonate; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; zinc dibromide; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.11.046

Reference yield:

: 41337-81-9
ethyl 6-(hydroxymethyl)pyridine-2-carboxylate

: 1416326-47-0
C₂₆H₁₈Cl₃FN₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane

2.1: ethylmagnesium bromide / dichloromethane

3.1: hydrogen; palladium on activated charcoal; zinc dibromide / ethyl acetate

4.1: potassium carbonate / ethanol

4.2: Reflux

5.1: acetic acid / toluene

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With palladium on activated charcoal; ethylmagnesium bromide; hydrogen; sulfur trioxide pyridine complex; potassium carbonate; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; zinc dibromide; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.11.046

Reference yield:

: 892663-03-5
ethyl 6-((5-chloro-2-hydroxyphenyl)methyl)-2-pyridinecarboxylate

: 1416326-47-0
C₂₆H₁₈Cl₃FN₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ethanol

1.2: Reflux

2.1: acetic acid / toluene

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.11.046