(2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF))

Base Information

• Chemical Name: (2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF))
• CAS No.: 1338066-13-9
• Molecular Formula: C₅₂H₅₄Cl₄Cr₂N₂O₄
• Molecular Weight: 1016.82
• Mol file: 1338066-13-9.mol

Synonyms:

Chemical Property of (2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF))

There total 1 articles about (2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

CrCl2(tetrahydrofuran)2 (15604-50-9) + ((2,6-diethylphenyl)imino)-acenaphthenone → (2,6-Et2C6H3-C12H6NO)(κ3N,O,O'-CrCl(THF))(μ-Cl)(μ-O)(κ2N',O-CrCl2(THF)) (1338066-13-9)

Guidance literature:

In dichloromethane; (N2); using Schlenk techniques; stirring of C12H6NO(2,6-Et2C6H3)2 and CrCl2(THF)2 for 6 h at 25°C; concn., decanting of mother liquor, washing with hexane, drying in vac.;elem. anal.;

DOI:10.1021/om200733e

upstream raw materials:

CrCl₂(tetrahydrofuran)2