C₅₂H₆₈O₁₀Si

Base Information

Chemical Name:C₅₂H₆₈O₁₀Si
CAS No.:1352816-10-4
Molecular Formula:C₅₂H₆₈O₁₀Si
Molecular Weight:881.191
Hs Code.:

C<sub>52</sub>H<sub>68</sub>O<sub>10</sub>Si

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Chemical Property of C₅₂H₆₈O₁₀Si

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Technology Process of C₅₂H₆₈O₁₀Si

There total 4 articles about C₅₂H₆₈O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352816-09-1
C₅₀H₆₆O₉Si

: 108-24-7
acetic anhydride

: 1352816-10-4
C₅₂H₆₈O₁₀Si

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-07-9
C₅₀H₆₄O₈Si

: 1352816-10-4
C₅₂H₆₈O₁₀Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: o-xylene / 20 h / 165 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

2.2: NaBO₃*4H₂O / 3 h / 20 °C

3.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C

With pyridine; dmap; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; o-xylene; 2.1: Hydroboration reaction;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-08-0
C₅₀H₆₄O₈Si

: 1352816-10-4
C₅₂H₆₈O₁₀Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

1.2: NaBO₃*4H₂O / 3 h / 20 °C

2.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C

With pyridine; dmap; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; 1.1: Hydroboration reaction;
DOI:10.1002/anie.201104681