C₁₈H₁₆ClNO₃

Base Information

Chemical Name:C₁₈H₁₆ClNO₃
CAS No.:1304134-13-1
Molecular Formula:C₁₈H₁₆ClNO₃
Molecular Weight:329.783
Hs Code.:

C<sub>18</sub>H<sub>16</sub>ClNO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₆ClNO₃

Chemical Property:

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Technology Process of C₁₈H₁₆ClNO₃

There total 4 articles about C₁₈H₁₆ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67865-74-1
N-phthaloyl-(3S)-3-amino-1-chloro-4-phenyl-2-butanone

: C₁₈H₁₆ClNO₃

: 1304134-13-1
C₁₈H₁₆ClNO₃

Guidance literature:: With isopropyl alcohol; In toluene; at 50 ℃; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 5123-55-7
Nα-phthaloyl-L-phenylalanine

: C₁₈H₁₆ClNO₃

: 1304134-13-1
C₁₈H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 °C / Inert atmosphere

2: dichloromethane; hexane / 25 h / 0 °C / Inert atmosphere

3: hydrogenchloride / dichloromethane; hexane; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

4: isopropyl alcohol / toluene / 50 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; isopropyl alcohol; N,N-dimethyl-formamide; In diethyl ether; hexane; dichloromethane; toluene; 4: Meerwein-Ponndorf-Verley Reduction;

Reference yield:

: 32150-91-7
phthaloyl-L-phenylalanyl chloride

: C₁₈H₁₆ClNO₃

: 1304134-13-1
C₁₈H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane; hexane / 25 h / 0 °C / Inert atmosphere

2: hydrogenchloride / dichloromethane; hexane; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

3: isopropyl alcohol / toluene / 50 °C / Inert atmosphere

With hydrogenchloride; isopropyl alcohol; In diethyl ether; hexane; dichloromethane; toluene; 3: Meerwein-Ponndorf-Verley Reduction;