3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

Base Information

Chemical Name:3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide
CAS No.:1383845-12-2
Molecular Formula:C₁₉H₂₀N₄O₂
Molecular Weight:336.393
Hs Code.:

Synonyms:

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Chemical Property of 3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

There total 7 articles about 3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24425-40-9
indan-5-amine

: 1383845-12-2
3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane

2.1: nitric acid; acetic anhydride / dichloromethane

3.1: hydrogenchloride / water / Reflux

4.1: diethyl ether / 1 h / 100 °C

4.2: 3 h / 50 - 110 °C

4.3: 3 h / 50 - 110 °C

5.1: tert.-butylnitrite; sulfuric acid / water; tert-butyl alcohol / 60 °C

6.1: trichlorophosphate / 3 h / Reflux

7.1: water; fluorine; acetonitrile / dichloromethane / 0.17 h / -15 - 0 °C / Inert atmosphere

8.1: triethylamine / 0 - 20 °C

With hydrogenchloride; tert.-butylnitrite; sulfuric acid; water; nitric acid; acetic anhydride; fluorine; triethylamine; acetonitrile; trichlorophosphate; In diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jm300123s

Reference yield:

: 52957-66-1
5-amino-6-nitroindane

: 1383845-12-2
3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethyl ether / 1 h / 100 °C

1.2: 3 h / 50 - 110 °C

1.3: 3 h / 50 - 110 °C

2.1: tert.-butylnitrite; sulfuric acid / water; tert-butyl alcohol / 60 °C

3.1: trichlorophosphate / 3 h / Reflux

4.1: water; fluorine; acetonitrile / dichloromethane / 0.17 h / -15 - 0 °C / Inert atmosphere

5.1: triethylamine / 0 - 20 °C

With tert.-butylnitrite; sulfuric acid; water; fluorine; triethylamine; acetonitrile; trichlorophosphate; In diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jm300123s

Reference yield:

: 55491-36-6
5-acetamino-6-nitro-indane

: 1383845-12-2
3-(methyl(phenethyl)amino)-7,8-dihydro-6H-indeno[5,6-e]-[1,2,4]triazine-1,4-dioxide

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / Reflux

2.1: diethyl ether / 1 h / 100 °C

2.2: 3 h / 50 - 110 °C

2.3: 3 h / 50 - 110 °C

3.1: tert.-butylnitrite; sulfuric acid / water; tert-butyl alcohol / 60 °C

4.1: trichlorophosphate / 3 h / Reflux

5.1: water; fluorine; acetonitrile / dichloromethane / 0.17 h / -15 - 0 °C / Inert atmosphere

6.1: triethylamine / 0 - 20 °C

With hydrogenchloride; tert.-butylnitrite; sulfuric acid; water; fluorine; triethylamine; acetonitrile; trichlorophosphate; In diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jm300123s