Technology Process of C26H24N2O4S
There total 5 articles about C26H24N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 18.33 h / 0 - 20 °C
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 5 h / 80 °C / Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; cesium fluoride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 0 - 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; cesium fluoride; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
3: Suzuki coupling;
DOI:10.1021/ml200024y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; cesium fluoride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 0 - 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; cesium fluoride; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane;
1: Suzuki coupling;
DOI:10.1021/ml200024y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 5 h / 80 °C / Inert atmosphere
2: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; cesium fluoride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 0 - 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; cesium fluoride; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane;
2: Suzuki coupling;
DOI:10.1021/ml200024y