C₂₇H₃₁N₄O₉P

Base Information

Chemical Name:C₂₇H₃₁N₄O₉P
CAS No.:1532523-70-8
Molecular Formula:C₂₇H₃₁N₄O₉P
Molecular Weight:586.538
Hs Code.:

C<sub>27</sub>H<sub>31</sub>N<sub>4</sub>O<sub>9</sub>P

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₁N₄O₉P

Chemical Property:

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Technology Process of C₂₇H₃₁N₄O₉P

There total 13 articles about C₂₇H₃₁N₄O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255860-30-0
1-((2R,3R,4R,5R)-3-allyl-4-(benzyloxy)-5-(benzyloxymethyl)-3-hydroxytetra-hydrofuran-2-yl)pyrimidine-2,4(1H,3H)-dione

: 1532523-70-8
C₂₇H₃₁N₄O₉P

Guidance literature:: Multi-step reaction with 10 steps

1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 2 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; water / 20 °C

3: pyridine / 2 h

4: sodium hydride / tetrahydrofuran / 2 h / 20 °C

5: palladium(II) hydroxide; hydrogen / tetrahydrofuran / 18 h / 25 °C / 775.74 Torr / Inert atmosphere

6: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 20 °C

7: dmap; triethylamine / acetonitrile / 2 h / 20 °C

8: ammonium hydroxide / 1.5 h / 20 °C

9: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

10: pyridine; 1-methyl-1H-imidazole / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; dmap; ammonium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; hydrogen; palladium(II) hydroxide; sodium hydride; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm4015422

Reference yield:

: C₃₃H₃₂N₂O₇

: 1532523-70-8
C₂₇H₃₁N₄O₉P

Guidance literature:: Multi-step reaction with 11 steps

1: methanol; sodium methylate

2: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 2 h / 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; water / 20 °C

4: pyridine / 2 h

5: sodium hydride / tetrahydrofuran / 2 h / 20 °C

6: palladium(II) hydroxide; hydrogen / tetrahydrofuran / 18 h / 25 °C / 775.74 Torr / Inert atmosphere

7: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 20 °C

8: dmap; triethylamine / acetonitrile / 2 h / 20 °C

9: ammonium hydroxide / 1.5 h / 20 °C

10: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

11: pyridine; 1-methyl-1H-imidazole / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; methanol; dmap; ammonium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; hydrogen; sodium methylate; palladium(II) hydroxide; sodium hydride; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm4015422

Reference yield:

: 1255860-31-1
1-[(2R,3R,4R,5R)-4-(benzyloxy)-5-(benzyloxy-methyl)-3-hydroxy-3-(2-hydroxyethyl)tetrahydrofuran-2-yl]pyrimidine-2,4(1H,3H)-dione

: 1532523-70-8
C₂₇H₃₁N₄O₉P

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / 2 h

2: sodium hydride / tetrahydrofuran / 2 h / 20 °C

3: palladium(II) hydroxide; hydrogen / tetrahydrofuran / 18 h / 25 °C / 775.74 Torr / Inert atmosphere

4: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 20 °C

5: dmap; triethylamine / acetonitrile / 2 h / 20 °C

6: ammonium hydroxide / 1.5 h / 20 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

8: pyridine; 1-methyl-1H-imidazole / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; dmap; ammonium hydroxide; tetrabutyl ammonium fluoride; hydrogen; palladium(II) hydroxide; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm4015422