Technology Process of C16H13F3O4S2
There total 4 articles about C16H13F3O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper diacetate; triethylamine / dichloromethane / 36 h / 20 °C / Inert atmosphere; Molecular sieve
2: potassium carbonate / methanol; acetonitrile / 1.17 h / 20 °C / Inert atmosphere; Cooling with ice
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice
4: thiourea / methanol / 18 h / 20 °C / Inert atmosphere
With
copper diacetate; potassium carbonate; triethylamine; thiourea; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; acetonitrile;
1: Suzuki coupling;
DOI:10.1021/ml300050b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol; acetonitrile / 1.17 h / 20 °C / Inert atmosphere; Cooling with ice
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice
3: thiourea / methanol / 18 h / 20 °C / Inert atmosphere
With
potassium carbonate; thiourea; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/ml300050b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice
2: thiourea / methanol / 18 h / 20 °C / Inert atmosphere
With
thiourea; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane;
DOI:10.1021/ml300050b
