C₁₉H₂₃NOS

Base Information

Chemical Name:C₁₉H₂₃NOS
CAS No.:1428366-61-3
Molecular Formula:C₁₉H₂₃NOS
Molecular Weight:313.464
Hs Code.:

Synonyms:

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Chemical Property of C₁₉H₂₃NOS

Chemical Property:

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Technology Process of C₁₉H₂₃NOS

There total 5 articles about C₁₉H₂₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428365-94-9
(R_s)-2-phenylpropyl-2-sulfinamide

: 1428366-61-3
C₁₉H₂₃NOS

Guidance literature:: Multi-step reaction with 2 steps

1: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

2: tetrahydrofuran / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo400354r

Reference yield:

: 94265-89-1
bis(1-methyl-1-phenylethyl)disulfide

: 1428366-61-3
C₁₉H₂₃NOS

Guidance literature:: Multi-step reaction with 5 steps

1.1: dihydrogen peroxide; (1S,2R)-1-(3,5-di-tert-butyl-2-hydroxybenzylideneamino)-2,3-dihydro-1H-inden-2-ol; bis(acetylacetonate)oxovanadium / water; acetone / 46 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4.1: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

5.1: tetrahydrofuran / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; n-butyllithium; bis(acetylacetonate)oxovanadium; (1S,2R)-1-(3,5-di-tert-butyl-2-hydroxybenzylideneamino)-2,3-dihydro-1H-inden-2-ol; tetrabutyl ammonium fluoride; dihydrogen peroxide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jo400354r

Reference yield:

: 1428366-11-3
C₁₈H₂₂OS₂

: 1428366-61-3
C₁₉H₂₃NOS

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

4.1: tetrahydrofuran / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo400354r