Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

Base Information

Chemical Name:Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester
CAS No.:188120-34-5
Molecular Formula:C₅₇H₆₃N₃O₆S₆
Molecular Weight:1078.54
Hs Code.:

Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

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Chemical Property of Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

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Technology Process of Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

There total 2 articles about Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81370-49-2,68198-62-9,75322-24-6,68182-93-4
cyclotriguaiacyclene

: 188120-34-5
Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / potassium carbonate / acetone / 8 h / Heating

2: 72 percent / acetonitrile / 8 h / Ambient temperature

With potassium carbonate; In acetone; acetonitrile;

Reference yield:

: 86534-12-5,123805-89-0,123805-90-3
(±)-2,7,12-trimethoxy-3,8,13-tris(2-propenyloxy)-10,15-dihydro-5Htribenzo[a,d,g]cyclononene

: 188120-34-5
Dimethyl-dithiocarbamic acid 3-[7,12-bis-(3-dimethylthiocarbamoylsulfanylmethyl-benzyloxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxymethyl]-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / triphenylphosphine, trimethylammonium formate, palladium(II) acetate / acetonitrile; H₂O / 2 h / Heating

2: 45 percent / potassium carbonate / acetone / 8 h / Heating

3: 72 percent / acetonitrile / 8 h / Ambient temperature

With palladium diacetate; trimethylamine-formic acid complex; potassium carbonate; triphenylphosphine; In water; acetone; acetonitrile;