tri-m-tolyl boron-pyridine

Base Information

Chemical Name:tri-m-tolyl boron-pyridine
CAS No.:75544-26-2
Molecular Formula:C₂₆H₂₆BN
Molecular Weight:363.31
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri-m-tolyl boron-pyridine

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Technology Process of tri-m-tolyl boron-pyridine

There total 1 articles about tri-m-tolyl boron-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 10325-82-3
m-tolyllithium

: 19287-45-7
diborane

: 75544-26-2
tri-m-tolyl boron-pyridine

Guidance literature:: With pyridine; copper(I) bromide; In not given; Li educt added to CuBr slurry in ether at 0°C under N2, reacted for 10 min, B2H6 soln. added, stirred for 18 h at room temp.; hydrolyzed with H2O and aq. NaOH, extd. with ether, ligand slight excess added to ether phase, stirred at room temp. for 12 h, concd. (vac.), solid recrystd. (ether/petroleum ether);
DOI:10.1016/S0022-328X(00)89999-4