diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate

Base Information

Chemical Name:diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate
CAS No.:150174-87-1
Molecular Formula:C₁₇H₂₉B₁₀NO₅
Molecular Weight:435.531
Hs Code.:

diethyl p-{1,2-dicarba-closo-dodecaboran<sup>(12)</sup>-1-yl}benzyl(formamido)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate

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Technology Process of diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate

There total 1 articles about diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 150174-85-9
1-{p-(alpha-bromo)tolyl}-1,2-dicarba-closo-dodecaborane

: 6326-44-9
diethyl 2-formylaminomalonate

: 150174-87-1
diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate

Guidance literature:: With sodium; sodium iodide; In ethanol; the malonate is added to a soln. of sodium in dry absolute alcohol and this is followed by borane-compd. and a few crystals of NaI, the mixt. is stored at room temp. for 2 days, heated to reflux for 2.5 h; evapn. to dryness, the residue is dissolved in ether, the soln. is washed with water and evaporated, the residue is purified by chromy. and then recrystallised from EtOH;

Reference yield: 89.0%

: 150174-87-1
diethyl p-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}benzyl(formamido)malonate

: 146490-19-9
4-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}phenylalanine

Guidance literature:: With hydrogenchloride; acetic acid; the borane-compd. is taken up in HCl and the mixt. allowed to reflux, after 20 min, acetic acid is introduced and reflux continued for 4 h; the mixt. is evaporated to dryness, the residue is crystallised from aq. EtOH;