N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

Base Information

Chemical Name:N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide
CAS No.:1463445-36-4
Molecular Formula:C₆₂H₄₈N₄O₁₂
Molecular Weight:1041.08
Hs Code.:

N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

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Chemical Property of N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

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Technology Process of N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

There total 2 articles about N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 31406-52-7
20,24-diamino-2,3,11,12-dibenzo-1,4,7,10,13,16-hexaoxacyclooctadeca-2,11-diene

: 72385-93-4
1-(p-tert-butylphenoxy)-4-benzoylamino-9,10-anthraquinone

: 1463445-36-4
N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

Guidance literature:: In benzene; at 20 ℃; UV-irradiation;
DOI:10.1007/s11172-012-0323-z

Reference yield:

: 32082-45-4
trans-di(nitrobenzo)-18-crown-6

: 1463445-36-4
N,N'-{10,10'-[(6,7,9,10,17,18,20,21-octahydrodibenzo-[b,k][1,4,7,10,13,16]hexaoxacyclooctadecine-2,13-diyl)di-imino]bis(4-hydroxy-9-oxo-9,10-dihydroanthracen-1-yl)}dibenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; palladium on activated charcoal / diethylene glycol dimethyl ether

2: benzene / 20 °C / UV-irradiation

With palladium on activated charcoal; hydrazine hydrate; In diethylene glycol dimethyl ether; benzene;
DOI:10.1007/s11172-012-0323-z