(2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate

Base Information

Chemical Name:(2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate
CAS No.:1414882-63-5
Molecular Formula:C₁₈H₂₃NO₃
Molecular Weight:301.386
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate

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Technology Process of (2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate

There total 2 articles about (2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 51944-67-3
N-benzyl-3-methylpropenamide

: 1414882-63-5
(2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate

Guidance literature:: With potassium hexafluorophosphate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate monohydrate; In 1,4-dioxane; water; acetic acid; at 100 ℃; for 18h; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c2cc36137j

Reference yield:

: 100-46-9
benzylamine

: 1414882-63-5
(2E,4Z)-n-butyl 6-benzylamino-4-methyl-6-oxohexa-2,4-dienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 0.08 h / 20 °C

2: potassium hexafluorophosphate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate monohydrate / 1,4-dioxane; water; acetic acid / 18 h / 100 °C / Inert atmosphere

With potassium hexafluorophosphate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper(II) acetate monohydrate; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; water; acetic acid; acetonitrile;
DOI:10.1039/c2cc36137j