C₅₂H₄₅BF₂N₄O₂

Base Information

Chemical Name:C₅₂H₄₅BF₂N₄O₂
CAS No.:1579250-79-5
Molecular Formula:C₅₂H₄₅BF₂N₄O₂
Molecular Weight:806.763
Hs Code.:

C<sub>52</sub>H<sub>45</sub>BF<sub>2</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₅₂H₄₅BF₂N₄O₂

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Technology Process of C₅₂H₄₅BF₂N₄O₂

There total 3 articles about C₅₂H₄₅BF₂N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1579250-78-4
C₅₉H₄₇BF₂N₄O₂

: 1579250-79-5
C₅₂H₄₅BF₂N₄O₂

Guidance literature:: With palladium 10% on activated carbon; hydrogen; at 20 ℃; for 4h; under 760.051 Torr;
DOI:10.1002/chem.201303868

Reference yield:

: C₂₁H₂₂N₂O₂

: 1579250-79-5
C₅₂H₄₅BF₂N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere

2: piperidine; acetic acid / toluene / 12 h / Dean-Stark; Reflux

3: palladium 10% on activated carbon; hydrogen / 4 h / 20 °C / 760.05 Torr

With piperidine; palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; In dichloromethane; toluene; 2: |Knoevenagel Condensation;
DOI:10.1002/chem.201303868

Reference yield:

: 1579250-77-3
C₂₁H₂₁BF₂N₂O₂

: 1579250-79-5
C₅₂H₄₅BF₂N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine; acetic acid / toluene / 12 h / Dean-Stark; Reflux

2: palladium 10% on activated carbon; hydrogen / 4 h / 20 °C / 760.05 Torr

With piperidine; palladium 10% on activated carbon; hydrogen; acetic acid; In toluene; 1: |Knoevenagel Condensation;
DOI:10.1002/chem.201303868