1,3-dithia-2-stibacyclopentane diphenyldithiophosphate

Base Information

• Chemical Name: 1,3-dithia-2-stibacyclopentane diphenyldithiophosphate
• CAS No.: 915950-39-9
• Molecular Formula: C₁₄H₁₄O₂PS₄Sb
• Molecular Weight: 495.252
• Mol file: 915950-39-9.mol

Synonyms:

Chemical Property of 1,3-dithia-2-stibacyclopentane diphenyldithiophosphate

Chemical Property:

Purity/Quality:

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Technology Process of 1,3-dithia-2-stibacyclopentane diphenyldithiophosphate

There total 1 articles about 1,3-dithia-2-stibacyclopentane diphenyldithiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

diphenyldithiophosphoric acid sodium salt + ethane-1,2-dithiolatoantimony(III) chloride (3741-30-8) → 1,3-dithia-2-stibacyclopentane diphenyldithiophosphate (915950-39-9)

Guidance literature:

In benzene; byproducts: NaCl; equimolar amt. of benezene soln. of Sb-compd. was added to thiophosphoric acid, reflux for ca. 5 h; cooling to room temp., ppt. was filtered off, solvent was removed in vac., recrystn. from CH2Cl2; elem. anal.;

DOI:10.1016/j.poly.2006.04.027

upstream raw materials:

ethane-1,2-dithiolatoantimony(III) chloride