C₁₄H₁₃N₃

Base Information

• Chemical Name: C₁₄H₁₃N₃
• CAS No.: 1330064-82-8
• Molecular Formula: C₁₄H₁₃N₃
• Molecular Weight: 223.277
• Mol file: 1330064-82-8.mol

Synonyms:

Chemical Property of C₁₄H₁₃N₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₃N₃

There total 3 articles about C₁₄H₁₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-1H-indazole (3176-63-4) → C14H13N3 (1330064-82-8)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide

2: tin(ll) chloride; hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate / dichloromethane; water / pH 9

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; caesium carbonate; tin(ll) chloride; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.02.034

Reference yield:

4-Fluoronitrobenzene (350-46-9,178603-76-4) → C14H13N3 (1330064-82-8)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide

2: tin(ll) chloride; hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate / dichloromethane; water / pH 9

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; caesium carbonate; tin(ll) chloride; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.02.034

Reference yield:

C14H11N3O2 (1438463-93-4) → C14H13N3 (1330064-82-8)

Guidance literature:

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; tin(ll) chloride; In dichloromethane; water; pH=9;

DOI:10.1016/j.bmcl.2013.02.034

upstream raw materials:

4-methyl-1H-indazole

C₁₄H₁₁N₃O₂

4-Fluoronitrobenzene

Downstream raw materials:

C₂₂H₁₆ClF₃N₄O