C₂₂H₂₃N₃O₅S

Base Information

Chemical Name:C₂₂H₂₃N₃O₅S
CAS No.:1435914-93-4
Molecular Formula:C₂₂H₂₃N₃O₅S
Molecular Weight:441.508
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₂H₂₃N₃O₅S

Chemical Property:

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Technology Process of C₂₂H₂₃N₃O₅S

There total 8 articles about C₂₂H₂₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₅N₃O₅S

: 1435914-93-4
C₂₂H₂₃N₃O₅S

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2013.04.023

Reference yield:

: 1252632-09-9
(2S,4R)-methyl 4-benzenesulfonyl-N-Boc-pyrrolidine-2-carboxylate

: 1435914-93-4
C₂₂H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h

2: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 0 - 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

4: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

With hydrogenchloride; water; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2013.04.023

Reference yield:

: 74844-91-0
1-tert-butyl 2-methyl (2S,4R)-4-hydroxy-1,2-pyrrolidinedicarboxylate

: 1435914-93-4
C₂₂H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine; triethylamine / tetrahydrofuran / 15 h / 70 °C

2: sodium hydride / tetrahydrofuran / 4.5 h / 0 - 50 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h

4: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h

5: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 0 - 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

7: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; sodium hydride; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.04.023