α-Methylzimtsaeureanilid

Base Information

• Chemical Name: α-Methylzimtsaeureanilid
• CAS No.: 71099-84-8
• Molecular Formula: C₁₆H₁₅NO
• Molecular Weight: 237.301
• Mol file: 71099-84-8.mol

Synonyms:

Chemical Property of α-Methylzimtsaeureanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-Methylzimtsaeureanilid

There total 2 articles about α-Methylzimtsaeureanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-3-phenylacryloyl chloride (38449-13-7,35086-87-4) + aniline (62-53-3) → α-Methylzimtsaeureanilid (71099-84-8,80818-45-7,71569-19-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.200900080

Reference yield:

→ α-Methylzimtsaeureanilid (71099-84-8,80818-45-7,71569-19-2)

Guidance literature:

α-Methylcinnamoylchlorid, Anilin;

Reference yield: 95.0%

propene (187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4) + α-Methylzimtsaeureanilid (71099-84-8,80818-45-7,71569-19-2) → C19H21NO (1351464-70-4)

Guidance literature:

With [(C₆H₆)(PCy₃)(CO)RuH]⁺*BF₄^?; In dichloromethane; at 70 ℃; for 14h;

DOI:10.1021/om201190v

upstream raw materials:

2-methyl-3-phenylacryloyl chloride

aniline

Downstream raw materials:

2-methyl-3,N-diphenyl-propionamide

C₁₆H₁₇NO

C₁₉H₂₁NO

(2E)-N,2-dimethyl-N,3-diphenylacrylamide