5-triphenylphosphoniopentanoate

Base Information

Chemical Name:5-triphenylphosphoniopentanoate
CAS No.:60633-16-1
Molecular Formula:C₂₃H₂₃O₂P
Molecular Weight:362.408
Hs Code.:

Synonyms:

Suppliers and Price of 5-triphenylphosphoniopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-triphenylphosphoniopentanoate

Chemical Property:

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Technology Process of 5-triphenylphosphoniopentanoate

There total 1 articles about 5-triphenylphosphoniopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60633-16-1
5-triphenylphosphoniopentanoate

Guidance literature:: y-Butyrolacton, Phosphoran 2 (R=H), THF;
DOI:10.1039/C39760000299

Reference yield:

: 60633-16-1
5-triphenylphosphoniopentanoate

: 130520-29-5
C₂₀H₂₅NO₇S

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Wittig coupling

2: 99 percent / toluene / 23 °C

3: 96 percent / LiOH / tetrahydrofuran; methanol; H₂O / 5 h / 23 °C

With lithium hydroxide; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1016/S0040-4039(00)97481-1

Reference yield:

: 60633-16-1
5-triphenylphosphoniopentanoate

: 130608-32-1
(Z)-7-[(1S,2S,3R,5R)-3-(Toluene-4-sulfonylamino)-6-oxa-bicyclo[3.1.0]hex-2-yl]-hept-5-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) sodium hexamethyldisilazane / 1) toluene, THF, -40 to 0 deg C, 2 h 2) 0 deg C

2: 96 percent / LiOH / methanol; H₂O; tetrahydrofuran / 4 h / 23 °C

With lithium hydroxide; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; water;
DOI:10.1016/S0040-4039(00)97481-1