C₁₈H₁₆BBrO₃

Base Information

Chemical Name:C₁₈H₁₆BBrO₃
CAS No.:1581276-40-5
Molecular Formula:C₁₈H₁₆BBrO₃
Molecular Weight:371.038
Hs Code.:

C<sub>18</sub>H<sub>16</sub>BBrO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₆BBrO₃

Chemical Property:

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Technology Process of C₁₈H₁₆BBrO₃

There total 4 articles about C₁₈H₁₆BBrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55718-76-8
2-chloro-1,3,2-benzodioxaborole

: 1581276-07-4
4-bromo-2-(hex-1-yn-1-yl)phenol

: 1581276-40-5
C₁₈H₁₆BBrO₃

Guidance literature:: 4-bromo-2-(hex-1-yn-1-yl)phenol; With sodium 2,2,2-trifluoroacetate; sodium hydride; In toluene; mineral oil; at 25 ℃; for 0.25h; Schlenk technique; Glovebox;

2-chloro-1,3,2-benzodioxaborole; In toluene; at 25 ℃; for 0.5h; Schlenk technique; Glovebox;
DOI:10.1021/ja500463p

Reference yield:

: 207115-22-8
4-bromo-2-iodophenol

: 1581276-40-5
C₁₈H₁₆BBrO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 1 h / 0 - 25 °C / Inert atmosphere

2.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 15 h / 25 °C / Inert atmosphere; Schlenk technique

3.1: potassium carbonate / methanol; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium hydride; sodium 2,2,2-trifluoroacetate / toluene; mineral oil / 0.25 h / 25 °C / Schlenk technique; Glovebox

4.2: 0.5 h / 25 °C / Schlenk technique; Glovebox

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium 2,2,2-trifluoroacetate; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
DOI:10.1021/ja500463p

Reference yield:

: 2-iodo-4-bromophenyl acetic acid

: 1581276-40-5
C₁₈H₁₆BBrO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 15 h / 25 °C / Inert atmosphere; Schlenk technique

2.1: potassium carbonate / methanol; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydride; sodium 2,2,2-trifluoroacetate / toluene; mineral oil / 0.25 h / 25 °C / Schlenk technique; Glovebox

3.2: 0.5 h / 25 °C / Schlenk technique; Glovebox

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium 2,2,2-trifluoroacetate; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; toluene; mineral oil;
DOI:10.1021/ja500463p