acetylglycyl>glycine ethyl ester

Base Information

Chemical Name:acetylglycyl>glycine ethyl ester
CAS No.:126116-59-4
Molecular Formula:C₂₅H₃₀N₂O₉
Molecular Weight:502.521
Hs Code.:

<N-<(6'-hydroxy-4,4'-dimethoxydihydrochalcone)-2'-yloxy>acetylglycyl>glycine ethyl ester

Synonyms:

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Chemical Property of acetylglycyl>glycine ethyl ester

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Technology Process of acetylglycyl>glycine ethyl ester

There total 4 articles about acetylglycyl>glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2087-41-4
glycyl glycine ethyl ester hydrochloride

: 126116-58-3
2'-(carboxy)methoxy-6'-hydroxy-4,4'-dimethoxydihydrochalcone

: 126116-59-4
acetylglycyl>glycine ethyl ester

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C, 1 h; 2.) RT;

Reference yield:

: 29424-96-2,102101-05-3,120851-84-5,137329-43-2,13238-06-7
naringenin-4',7-dimethyl ether

: 126116-59-4
acetylglycyl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 86.1 percent / Et₃N, H₂ / 10percent Pd/C / ethyl acetate / 4 h / Ambient temperature

2: 54.5 percent / K₂CO₃ / dimethylformamide / 72 h / Ambient temperature

3: 82.6 percent / 5percent KOH / 6 h / Ambient temperature

4: 75 percent / Et₃N, diethylphosphorocyanidate (DEPC) / dimethylformamide / 1.) 0 deg C, 1 h; 2.) RT

With potassium hydroxide; diethyl cyanophosphonate; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 35241-54-4
2',6'-dihydroxy-4',4-dimethoxy-dihydrochalcone

: 126116-59-4
acetylglycyl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 54.5 percent / K₂CO₃ / dimethylformamide / 72 h / Ambient temperature

2: 82.6 percent / 5percent KOH / 6 h / Ambient temperature

3: 75 percent / Et₃N, diethylphosphorocyanidate (DEPC) / dimethylformamide / 1.) 0 deg C, 1 h; 2.) RT

With potassium hydroxide; diethyl cyanophosphonate; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;