2--2',5-dichlorbenzophenon

Base Information

• Chemical Name: 2--2',5-dichlorbenzophenon
• CAS No.: 50436-56-1
• Molecular Formula: C₃₂H₂₄Cl₂N₂O₅
• Molecular Weight: 587.459

Synonyms:

Chemical Property of 2--2',5-dichlorbenzophenon

Chemical Property:

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Technology Process of 2--2',5-dichlorbenzophenon

There total 2 articles about 2--2',5-dichlorbenzophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.3%

1-chloroethyl benzyl ether (50436-46-9) + N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetamide (50436-53-8) → 2--2',5-dichlorbenzophenon (50436-56-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1248/cpb.30.1477

Reference yield:

→ 2--2',5-dichlorbenzophenon (50436-56-1)

Guidance literature:

Benzyl-1-chlorethylether, 2-Phthalimidoacetamido-2',5'-dichlorbenzophenon, NaH;

Reference yield: 53.5%

2--2',5-dichlorbenzophenon (50436-56-1) → 1-(1-benzyloxy-ethyl)-7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepin-2-one (50436-45-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1248/cpb.30.1477

upstream raw materials:

1-chloroethyl benzyl ether

N-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetamide

Downstream raw materials:

1-(1-benzyloxy-ethyl)-7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepin-2-one

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