bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride

Base Information

Chemical Name:bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride
CAS No.:496854-22-9
Molecular Formula:C₉H₂₂Cl₅OSi₂Sn₂*C₃₆H₃₀NP₂
Molecular Weight:1155.72
Hs Code.:

bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride

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Chemical Property of bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride

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Technology Process of bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride

There total 1 articles about bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 496854-18-3
1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 496854-22-9
bis(triphenylphosphoranylidene)ammonium-1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane chloride

Guidance literature:: In dichloromethane; under Ar atm. to soln. 1,1,5,5-tetrachloro-7,7,9,9-tetramethyl-7,9-disila-1,5-distanna-8-oxacyclodecane in CH2Cl2 was added dropwise PPNCl and stirred at room temp. for 10 min; solvent was removed in vacuo; elem. anal.;
DOI:10.1021/om020740b