tri-p-tolylantimony bis(cyclohexanone oximate)

Base Information

Chemical Name:tri-p-tolylantimony bis(cyclohexanone oximate)
CAS No.:78989-73-8
Molecular Formula:C₃₃H₄₁N₂O₂Sb
Molecular Weight:619.451
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri-p-tolylantimony bis(cyclohexanone oximate)

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Technology Process of tri-p-tolylantimony bis(cyclohexanone oximate)

There total 3 articles about tri-p-tolylantimony bis(cyclohexanone oximate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-64-1
cyclohexanone-oxime

: 13328-67-1,51017-91-5
penta(p-tolyl)antimony(V)

: 78989-73-8
tri-p-tolylantimony bis(cyclohexanone oximate)

Guidance literature:: In toluene; byproducts: CH3C6H5; mixt. (1:2) heated for 1 h at 90°C; crystn. (toluene-petroleum ether);
DOI:10.1007/s11176-005-0041-4

Reference yield:

: 100-64-1
cyclohexanone-oxime

: 594-31-0,34716-91-1,20265-29-6
triphenylantimony dichloride

: 78989-73-8
(CH₃(C₆H₄))3Sb(ONC(CH₂)5)2

Guidance literature:: With triethylamine; In benzene; byproducts: NH(Et)3Cl; triorganoantimony dihalide, oxime, and triethylamine are stirred together in benzene at room temp. for ca. 1 h; reaction mixt. refluxed for ca.3 h; triethylamine hydrohalide filtered off; concn. in vac.; recrystn. from benzene/petroleum-ether; elem. anal.;

Reference yield:

: 100-64-1
cyclohexanone-oxime

: 20265-30-9
triphenylantimony dibromide

: 78989-73-8
(CH₃(C₆H₄))3Sb(ONC(CH₂)5)2

Guidance literature:: With triethylamine; In benzene; byproducts: NH(Et)3Br; triorganoantimony dihalide, oxime, and triethylamine are stirred together in benzene at room temp. for ca. 1 h; reaction mixt. refluxed for ca.3 h; triethylamine hydrohalide filtered off; concn. in vac.; recrystn. from benzene/petroleum-ether; elem. anal.;