hexakis(cyclo-hexylgermasesquioxane)

Base Information

Chemical Name:hexakis(cyclo-hexylgermasesquioxane)
CAS No.:121772-30-3
Molecular Formula:C₃₆H₆₆Ge₆O₉
Molecular Weight:1078.45
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexakis(cyclo-hexylgermasesquioxane)

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Technology Process of hexakis(cyclo-hexylgermasesquioxane)

There total 2 articles about hexakis(cyclo-hexylgermasesquioxane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 13892-15-4
cyclohexyltrichlorogermane

: 1310-73-2
sodium hydroxide

: 121772-30-3
hexakis(cyclo-hexylgermasesquioxane)

Guidance literature:: In water; aq. NaOH was added to stirred soln. of Ge-compound in xylene, heated to reflux for 3 h; organic layer was washed with water, aq. phase was extd. with xylene, dried over MgSO4, evapd., recrystd. from Et2O; elem. anal.;
DOI:10.1016/S0022-328X(02)02157-5

Reference yield: 60.0%

: 7732-18-5
water

: 13892-15-4
cyclohexyltrichlorogermane

: 121772-30-3
hexakis(cyclo-hexylgermasesquioxane)

Guidance literature:: With aq. NaOH; In xylene; Ge compd. reacted with aq. NaOH in xylene at 130-140°C for 3 h; concd., crystd. from pentane;
DOI:10.1246/cl.2002.1124