oxovanadium(IV) cyclohexyl dithiocarboxylate

Base Information

• Chemical Name: oxovanadium(IV) cyclohexyl dithiocarboxylate
• CAS No.: 124659-68-3
• Molecular Formula: C₁₄H₂₂OS₄V
• Molecular Weight: 385.534
• Mol file: 124659-68-3.mol

Synonyms:

Chemical Property of oxovanadium(IV) cyclohexyl dithiocarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oxovanadium(IV) cyclohexyl dithiocarboxylate

There total 1 articles about oxovanadium(IV) cyclohexyl dithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vanadyl(IV) sulphate pentahydrate + potassium cyclohexyldithiocarboxylate (74670-41-0) → oxovanadium(IV) cyclohexyl dithiocarboxylate (124659-68-3)

Guidance literature:

In water; pH=4-5; dried over P4O10 under N2; elem. anal. after decompn. by heating with concd. HNO3-H2SO4 mixt. (1:1);

Reference yield: 65.0%

morpholine (110-91-8,99108-56-2) + oxovanadium(IV) cyclohexyl dithiocarboxylate (124659-68-3) → (morpholino)bis(cyclohexyldithiocarboxylato)oxovanadium(IV) (150390-71-9)

Guidance literature:

In further solvent(s); dissolution of oxovanadium complex in morpholine by continous stirring for 3 h at room temp.; cooling for 24 h, sepn. by filtn. in vacuo, drying over P4O10 in a N2 atmosphere, elem. anal.;

Reference yield: 65.0%

oxovanadium(IV) cyclohexyl dithiocarboxylate (124659-68-3) + cyclohexylamine (108-91-8,157973-60-9) → (cyclohexylamino)bis(cyclohexyldithiocarboxylato)oxovanadium(IV) (150430-74-3)

Guidance literature:

In further solvent(s); dissolution of oxovanadium complex in cyclohexylamine by continous stirring for 3 h at room temp.; cooling for 24 h, sepn. by filtn. in vacuo, drying over P4O10 in a N2 atmosphere, elem. anal.;

upstream raw materials:

potassium cyclohexyldithiocarboxylate

Downstream raw materials:

(morpholino)bis(cyclohexyldithiocarboxylato)oxovanadium(IV)

(cyclohexylamino)bis(cyclohexyldithiocarboxylato)oxovanadium(IV)