[(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl

Base Information

Chemical Name:[(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl
CAS No.:885462-53-3
Molecular Formula:C₂₇H₂₅MnO₃P₂
Molecular Weight:514.379
Hs Code.:

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Chemical Property of [(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl

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Technology Process of [(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl

There total 1 articles about [(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16853-85-3
lithium aluminium tetrahydride

: 885462-48-6,885462-50-0,255380-08-6
[(η(5)-2-formyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl

: 885462-55-5,255380-10-0,885462-53-3
[(η(5)-2-hydroxymethyl-3,4-dimethylphospholyl)(triphenylphosphine)]manganesedicarbonyl

Guidance literature:: In tetrahydrofuran; N2-atmosphere; 0.25 eqiuv. of LiAlH4; addn. of 1 M soln. of LiAlH4 to cooled soln. of Mn-compd. (-50°C), warming to room temp.; hydrolysis, etxn. to CH2Cl2, chromy. (SiO2, CH2Cl2/EtOAc 90/10); elem. anal.;
DOI:10.1021/om9904596