C₂₅H₂₈N₂O₂

Base Information

Chemical Name:C₂₅H₂₈N₂O₂
CAS No.:651006-23-4
Molecular Formula:C₂₅H₂₈N₂O₂
Molecular Weight:388.51
Hs Code.:

C<sub>25</sub>H<sub>28</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₂₈N₂O₂

Chemical Property:

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Technology Process of C₂₅H₂₈N₂O₂

There total 17 articles about C₂₅H₂₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 651006-22-3
C₂₅H₂₆N₂O₂

: 651006-23-4
C₂₅H₂₈N₂O₂

Guidance literature:: With diisobutylaluminium hydride;
DOI:10.1039/b310274b

Reference yield:

: 66087-97-6
(2S)-3-(2-Indolyl)-2-(tosylamino)propyl toluene-p-sulfonate

: 651006-23-4
C₂₅H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 13 steps

1: 88 percent / Na; NH₃ / tetrahydrofuran / 0.5 h

2: 3 Angstroem molecular sieves / 24 h

3: 80 percent / TFA / CH₂Cl₂ / 6 h / -78 - 20 °C

4: 75 percent / 70 °C

5: 87 percent / NaH / 0 °C

6: 96 percent / TBAF

7: 82 percent / NaH

8: LiNEt₂ / tetrahydrofuran / -78 °C

9: LiBH₄

10: 63 percent / TsOH*H₂₀ / tetrahydrofuran / Heating

11: 54 percent / DIBAL-H

With lithium borohydride; 3 A molecular sieve; lithium diethylamide; tetrabutyl ammonium fluoride; ammonia; sodium; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 4: Pictet-Spengler reaction / 8: Swern oxidation / 9: Wittig reaction / 10: Michael reaction;
DOI:10.1039/b310274b

Reference yield:

: 66087-99-8
(3S)-3-amino-4-(1H-indol-3-yl)butanenitrile

: 651006-23-4
C₂₅H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 11 steps

1: 3 Angstroem molecular sieves / 24 h

2: 80 percent / TFA / CH₂Cl₂ / 6 h / -78 - 20 °C

3: 75 percent / 70 °C

4: 87 percent / NaH / 0 °C

5: 96 percent / TBAF

6: 82 percent / NaH

7: LiNEt₂ / tetrahydrofuran / -78 °C

8: LiBH₄

9: 63 percent / TsOH*H₂₀ / tetrahydrofuran / Heating

10: 54 percent / DIBAL-H

With lithium borohydride; 3 A molecular sieve; lithium diethylamide; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 2: Pictet-Spengler reaction / 6: Swern oxidation / 7: Wittig reaction / 8: Michael reaction;
DOI:10.1039/b310274b