Technology Process of C17H16O3S2
There total 4 articles about C17H16O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium hexamethyldisilazane / tetrahydrofuran / 20 h / 0 °C
2: hydrogenchloride / tetrahydrofuran; water / Reflux
3: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C
4: sodium tetrahydroborate / methanol / 0.5 h / 0 °C
With
hydrogenchloride; sodium tetrahydroborate; lithium hexamethyldisilazane; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride;
In
tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1002/adsc.201300250
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / tetrahydrofuran; water / Reflux
2: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C
3: sodium tetrahydroborate / methanol / 0.5 h / 0 °C
With
hydrogenchloride; sodium tetrahydroborate; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride;
In
tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1002/adsc.201300250