C₂₆H₂₆O₁₂

Base Information

Chemical Name:C₂₆H₂₆O₁₂
CAS No.:917113-34-9
Molecular Formula:C₂₆H₂₆O₁₂
Molecular Weight:530.485
Hs Code.:

C<sub>26</sub>H<sub>26</sub>O<sub>12</sub>

Synonyms:

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Chemical Property of C₂₆H₂₆O₁₂

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Technology Process of C₂₆H₂₆O₁₂

There total 12 articles about C₂₆H₂₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 917113-20-3
C₃₀H₃₆O₁₅

: 917113-34-9
C₂₆H₂₆O₁₂

Guidance literature:: With 4 A molecular sieve; trifluoroacetic anhydride; In 1,2-dichloro-ethane; at 20 ℃; for 1h;
DOI:10.1021/ja066621v

Reference yield:

: 917113-23-6
C₁₇H₂₇BrO₆Si

: 917113-34-9
C₂₆H₂₆O₁₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: 90 percent / Me₄NBH(OAc)3; AcOH / acetonitrile / 24 h / 0 °C

2.1: 85 percent / 2,4,6-collidine / CH₂Cl₂ / 8 h / 5 °C

3.1: 95 percent / Super-Hydride / 1,2-dichloro-ethane; tetrahydrofuran / 0.5 h / 60 °C

4.1: 90 percent / K-10 clay / CH₂Cl₂ / 4 h / 20 °C

5.1: 70 percent / AsPh₃; CuCl; DIEA / Pd₂(dba)3 / acetonitrile / 4 h / 70 °C

6.1: 80 percent / Super-Hydride / tetrahydrofuran / 1 h / -78 °C

7.1: Ti(iPrO)4 / CH₂Cl₂ / 0.5 h / 20 °C

7.2: 60 percent / CH₂Cl₂ / 10 h / 20 °C

8.1: 140 mg / pyridine / 2 h / 20 °C

9.1: 78 mg / Et₃N-3HF / acetonitrile / 12 h / 20 °C

10.1: 72 mg / N-methylmorpholine N-oxide / tetrapropylammonium perruthenate / CH₂Cl₂ / 0.33 h / 20 °C

11.1: 64 mg / NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s); H₂O / 12 h / 20 °C

12.1: 90 percent / TFAA; 4 Angstroem molecular sieves / 1,2-dichloro-ethane / 1 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate; triphenyl-arsane; 4 A molecular sieve; K-10 clay; lithium triethylborohydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; copper(l) chloride; tetramethylammonium triacetoxyborohydride; tetrapropylammonium perruthennate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; tert-butyl alcohol; 5.1: Stille cross-coupling / 12.1: Friedel-Crafts annulation;
DOI:10.1021/ja066621v

Reference yield:

: 917113-37-2
C₁₇H₂₉BrO₆Si

: 917113-34-9
C₂₆H₂₆O₁₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 85 percent / 2,4,6-collidine / CH₂Cl₂ / 8 h / 5 °C

2.1: 95 percent / Super-Hydride / 1,2-dichloro-ethane; tetrahydrofuran / 0.5 h / 60 °C

3.1: 90 percent / K-10 clay / CH₂Cl₂ / 4 h / 20 °C

4.1: 70 percent / AsPh₃; CuCl; DIEA / Pd₂(dba)3 / acetonitrile / 4 h / 70 °C

5.1: 80 percent / Super-Hydride / tetrahydrofuran / 1 h / -78 °C

6.1: Ti(iPrO)4 / CH₂Cl₂ / 0.5 h / 20 °C

6.2: 60 percent / CH₂Cl₂ / 10 h / 20 °C

7.1: 140 mg / pyridine / 2 h / 20 °C

8.1: 78 mg / Et₃N-3HF / acetonitrile / 12 h / 20 °C

9.1: 72 mg / N-methylmorpholine N-oxide / tetrapropylammonium perruthenate / CH₂Cl₂ / 0.33 h / 20 °C

10.1: 64 mg / NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s); H₂O / 12 h / 20 °C

11.1: 90 percent / TFAA; 4 Angstroem molecular sieves / 1,2-dichloro-ethane / 1 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate; triphenyl-arsane; 4 A molecular sieve; K-10 clay; lithium triethylborohydride; 4-methylmorpholine N-oxide; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; copper(l) chloride; tetrapropylammonium perruthennate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; tert-butyl alcohol; 4.1: Stille cross-coupling / 11.1: Friedel-Crafts annulation;
DOI:10.1021/ja066621v