N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

Base Information

Chemical Name:N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide
CAS No.:94283-89-3
Molecular Formula:C₂₀H₂₄BrNO₄
Molecular Weight:422.319
Hs Code.:

Synonyms:

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Chemical Property of N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

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Technology Process of N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

There total 6 articles about N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94283-73-5
3-hydroxy-4-isopropoxy benzaldehyde

: 94283-89-3
N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / pyridine / 18 h

2: 50 percent / lithium tetrakis(N-dihydropyridyl)aluminate / pyridine / 48 h / 0 °C

3: 83 percent / pyridine, SOCl₂ / diethyl ether / 0.33 h / Ambient temperature

4: 95 percent / dimethylsulfoxide / 18 h / Ambient temperature

5: 100 percent / BF₃*OEt₂, NaBH₄ / tetrahydrofuran / 6 h / Ambient temperature

6: 75 percent / decahydronaphthalene / 2.5 h / Heating

7: 100 percent / KOH / dimethylformamide; methanol / 3 h / 70 °C

With pyridine; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; Lithium tetrakis(N-dihydropyridyl)aluminate; boron trifluoride diethyl etherate; In tetrahydrofuran; pyridine; methanol; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; decalin;

Reference yield:

: 94283-78-0
4-isopropoxy-3-tosyloxybenzyl chloride

: 94283-89-3
N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / dimethylsulfoxide / 18 h / Ambient temperature

2: 100 percent / BF₃*OEt₂, NaBH₄ / tetrahydrofuran / 6 h / Ambient temperature

3: 75 percent / decahydronaphthalene / 2.5 h / Heating

4: 100 percent / KOH / dimethylformamide; methanol / 3 h / 70 °C

With potassium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; decalin;

Reference yield:

: 94283-76-8
4-isopropoxy-3-tosyloxybenzylalcohol

: 94283-89-3
N-(3-hydroxy-4-isopropoxyphenethyl)-2-(2-bromo-6-methoxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / pyridine, SOCl₂ / diethyl ether / 0.33 h / Ambient temperature

2: 95 percent / dimethylsulfoxide / 18 h / Ambient temperature

3: 100 percent / BF₃*OEt₂, NaBH₄ / tetrahydrofuran / 6 h / Ambient temperature

4: 75 percent / decahydronaphthalene / 2.5 h / Heating

5: 100 percent / KOH / dimethylformamide; methanol / 3 h / 70 °C

With pyridine; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; decalin;