DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane

Base Information

• Chemical Name: DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane
• CAS No.: 1123889-70-2
• Molecular Formula: C₁₀H₁₂Cl₃GeNO₂
• Molecular Weight: 357.16
• Mol file: 1123889-70-2.mol

Synonyms:

Chemical Property of DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane

There total 1 articles about DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

N,N-dimethyl-2-phenyl-2-(trimethylsilyloxy)acetamide (917077-20-4) + germaniumtetrachloride (10038-98-9) → DL-[1-(dimethylcarbamoyl)-1-phenylmethoxy]trichlorogermane (1122104-09-9,1123889-70-2)

Guidance literature:

With Et₃N; In benzene; byproducts: Me3SiCl; GeCl4 added dropwise to mixt. of Si compd., Et3N and benzene; stirred for 24 h; diluted with o-xylene; refluxed for a short time; hot soln. filtered; cooled; crystals collected;

DOI:10.1016/j.jorganchem.2008.10.026

upstream raw materials:

N,N-dimethyl-2-phenyl-2-(trimethylsilyloxy)acetamide

germaniumtetrachloride