1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium

Base Information

• Chemical Name: 1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium
• CAS No.: 824984-43-2
• Molecular Formula: C₂₄H₂₀SiV
• Molecular Weight: 387.45

Synonyms:

Chemical Property of 1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium

Chemical Property:

Purity/Quality:

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Technology Process of 1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium

There total 1 articles about 1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

trovacene + diphenylsilyl dichloride (80-10-4) → 1,8-diphenylsilanediyl(η(7)-cycloheptatrienyl)(η(5)-cyclopentadienyl)vanadium (824984-43-2)

Guidance literature:

With nBuLi; Me₂NCH₂CH₂NMe₂; In diethyl ether; hexane; byproducts: LiCl; excess of nBuLi (1.6 M in hexane) and N-compd. were dropwise added to Et2O soln. of V-compd., reflux for 4 h, 1 equiv. of Si-compd. was added at-20 °C in petroleum ether in 2 h, stirring at room temp overnigh t; soln. was filtered, stored at -20 °C, elem. anal.;

DOI:10.1002/zaac.200400247

upstream raw materials:

diphenylsilyl dichloride

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