28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile

Base Information

• Chemical Name: 28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile
• CAS No.: 933787-55-4
• Molecular Formula: C₃₇H₅₃NO₃
• Molecular Weight: 559.833

Synonyms:

Chemical Property of 28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile

Chemical Property:

Purity/Quality:

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Technology Process of 28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile

There total 1 articles about 28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

28-benzoyloxy-3,4-secolup-4(23)-ene-3-nitrile → 28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile (933787-55-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 4 ℃; for 16h;

DOI:10.1135/cccc20061131

Reference yield: 53.0%

28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile (933787-55-4) → 3-oxo-24-norlupan-28-yl benzoate + 3,24-dioxolupan-28-yl benzoate

Guidance literature:

28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile; In toluene; for 2h; Heating;

With hydrogenchloride; In toluene; for 0.5h; Further stages.; Heating;

DOI:10.1135/cccc20061131

Reference yield:

28-benzoyloxy-4,23-epoxy-3,4-secolupane-3-nitrile (933787-55-4) → 3-oxo-24-norlupan-28-yl benzoate + 3-oxo-23-norlupan-28-yl benzoate + 3,24-dioxolupan-28-yl benzoate

Guidance literature:

With boron trifuoride diethyl etherate; In toluene; for 2h; Title compound not separated from byproducts.; Heating;

DOI:10.1135/cccc20061131

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