CpRu(1,2-bis(diphenylphosphino)ethane)CN

Base Information

Chemical Name:CpRu(1,2-bis(diphenylphosphino)ethane)CN
CAS No.:90444-04-5
Molecular Formula:C₃₂H₂₉NP₂Ru
Molecular Weight:590.606
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CpRu(1,2-bis(diphenylphosphino)ethane)CN

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Technology Process of CpRu(1,2-bis(diphenylphosphino)ethane)CN

There total 5 articles about CpRu(1,2-bis(diphenylphosphino)ethane)CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: chlorocyclopentadienylbis(triphenylphosphine)ruthenium(II)

: 90444-04-5
CpRu(1,2-bis(diphenylphosphino)ethane)CN

Guidance literature:: With KCN; In ethanol; water; Ru complex and 10 to 20 fold excess of KCN dissolved in 95% ethanol, heated at reflux for about 12 h, cooled; evapd. in vac., extd. with CH2Cl2, filtered, concd., pptd. ba adding 95% ethanol or hexane, collected by filtration, dried in vac.;

Reference yield:

: 204455-85-6
(C₅H₅)Ru((C₆H₅)2P(CH₂)2P(C₆H₅)2)CNH⁽¹⁺⁾*CF₃SO₃^(1-)=[(C₅H₅)Ru((C₆H₅)2P(CH₂)2P(C₆H₅)2)CNH]CF₃SO₃

: 90444-04-5
CpRu(1,2-bis(diphenylphosphino)ethane)CN

Guidance literature:: With diphenylguanidine; In not given; byproducts: diphenylguanidinium triflate; inert atmosphere; equimolar amts.; chromy. (Al2O3, CH2Cl2);
DOI:10.1021/ic971124o