ReCl(CO)3(P(CH₃)(C₆H₅)2)2

Base Information

Chemical Name:ReCl(CO)3(P(CH₃)(C₆H₅)2)2
CAS No.:118456-59-0
Molecular Formula:C₂₉H₂₆ClO₃P₂Re
Molecular Weight:706.131
Hs Code.:

ReCl(CO)3(P(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)2)2

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Suppliers and Price of ReCl(CO)3(P(CH₃)(C₆H₅)2)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of ReCl(CO)3(P(CH₃)(C₆H₅)2)2

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of ReCl(CO)3(P(CH₃)(C₆H₅)2)2

There total 2 articles about ReCl(CO)3(P(CH₃)(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 23136-99-4,80656-01-5
mer-[ReCl₃(CH₃P(C₆H₅)2)3]

: 118456-59-0,26553-95-7,27990-72-3
ReCl(CO)3(P(CH₃)(C₆H₅)2)2

Guidance literature:: With carbon monoxide; In benzene; CO atmosphere, stirring reactn. mixt. at 50°C (3 h); filtration, concn., pptn. by addn. of MeOH; elem. anal.;

Reference yield: 10.0%

: 14285-68-8
decacarbonyldirhenium⁽⁰⁾

: 1486-28-8
diphenyl(methyl)phosphine

: Re₂(CO)8(P(C₆H₅)2(CH₃))2

: 118456-59-0,26553-95-7,27990-72-3
fac-(ReCl(CO)3(PMePh₂)2)

: 101311-28-8,135682-06-3,32025-89-1
(Re₂(CO)9(P(CH₃)(C₆H₅)2))

Guidance literature:: With NMe₃O*2H₂O; In methanol; dichloromethane; to a soln. of Re2(CO)10 in CH2Cl2 PMePh2 is added; a soln. of NMe3O*2H2O in MeOH added; soln. warmed at 40°C for 8 h;; products isolated by preparative layer chromy., extd. with CH2Cl2 and recrystd. from CH2Cl2-pentane soln.; elem. anal.;;
DOI:10.1039/DT9850002277