acetylC₆H₄C₆H₄-0-carborane

Base Information

Chemical Name:acetylC₆H₄C₆H₄-0-carborane
CAS No.:65062-95-5
Molecular Formula:C₁₆H₂₂B₁₀O
Molecular Weight:338.46
Hs Code.:

acetylC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>-0-carborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetylC₆H₄C₆H₄-0-carborane

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Technology Process of acetylC₆H₄C₆H₄-0-carborane

There total 1 articles about acetylC₆H₄C₆H₄-0-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 17702-41-9
nido-decaborane

: 1086595-75-6
1-(4'-ethynyl-[1,1'-biphenyl]-4-yl)ethan-1-one

: 65062-95-5
acetylC₆H₄C₆H₄-0-carborane

Guidance literature:: In toluene; acetonitrile; (Ar); reflux of B10H14 in MeCN for 3 h, cooling to room temp., addn. of CH3COC6H4C6H4CCH in toluene, reflux at 90-100°C for 20 h; filtration, concn., chromy. on silica with 10% ethyl acetate in hexane; elem. anal.;
DOI:10.1021/ic200010q

Reference yield: 83.0%

: 88519-50-0
1,2-bis[4-(4'-acetylphenoxy)phenyl]-o-carborane

: 65062-95-5
acetylC₆H₄C₆H₄-0-carborane

: C₆H₃(C₁₂H₈C₂B₁₀H₁₁)C₆H₄OC₆H₄C₂B₁₀H₁₀C₆H₄OC₆H₄

Guidance literature:: With hydrogenchloride; orthoformic acid triethyl ester; In not given; react. of MeCOC6H4C6H4C2B10H11 with (MeCOC6H4OC6H4)2C2B10H10 in the presence of HC(OEt)2 by passing dry hydrogen chloride, heating at 400°C; (according to: V. N. Kalinin et al., Dokl. Akad. Nauk SSSR, 236, 367-370 (1977).); pptn. by add. of EtOH;