(CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)

Base Information

Chemical Name:(CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)
CAS No.:90444-02-3
Molecular Formula:C₂₆H₁₉FeMnN₂O₇
Molecular Weight:582.231
Hs Code.:

(CO)3Fe(C<sub>6</sub>H<sub>5</sub>CHCHCHCHC<sub>3</sub>H<sub>3</sub>N<sub>2</sub>(COCH<sub>3</sub>)C<sub>5</sub>H<sub>4</sub>Mn(CO)3)

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Suppliers and Price of (CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)

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Technology Process of (CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)

There total 1 articles about (CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 73523-69-0,90528-30-6
(CO)3Fe(C₆H₅CHCHCHCHCHCHCOC₅H₄Mn(CO)3)

: 7803-57-8,79785-97-0
hydrazine hydrate

: 90444-02-3
(CO)3Fe(C₆H₅CHCHCHCHC₃H₃N₂(COCH₃)C₅H₄Mn(CO)3)

Guidance literature:: With acetic acid anhydride; In ethanol; N2H4*H2O in alcohol was added to the Fe-complex, mixt. was stirred for 5 h at room temp., the excess of N2H4 was neutralized with glacial AcOH,Ac2O was added, mixt. was heated for 15 min; only single diastereomer was obtained; reaction mixt. was cooled, neutralized with Na2CO3, extd. with benzene,the product was purified by chromy. on SiO2 (eluent 1:1.5 petroleum ether-ether) and crystn. from aq. alcohol; elem. anal.;
DOI:10.1016/S0022-328X(00)99143-5