cis-(Ru(bpy)2(p-CH₂-cinn)2)(PF₆)2

Base Information

• Chemical Name: cis-(Ru(bpy)2(p-CH₂-cinn)2)(PF₆)2
• CAS No.: 85661-52-5
• Molecular Formula: C₅₀H₄₄N₈O₂Ru*2F₆P
• Molecular Weight: 1179.95

Synonyms:

Chemical Property of cis-(Ru(bpy)2(p-CH₂-cinn)2)(PF₆)2

Chemical Property:

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Technology Process of cis-(Ru(bpy)2(p-CH₂-cinn)2)(PF₆)2

There total 1 articles about cis-(Ru(bpy)2(p-CH₂-cinn)2)(PF₆)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ammonium hexafluorophosphate + cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate + N-(4-pyridylmethyl)cinnamamide (85649-71-4) → cis-(Ru(bpy)2(p-CH2-cinn)2)(PF6)2 (85661-52-5)

Guidance literature:

In ethanol; water; to soln. containing EtOH, water and 8-10 excess p-CH2-cinn deoxygenatedwith N2 for 20 min added cis-Ru(bpy)2Cl2*2H2O, mixt. refluxed under N2 for 18-24 h, reduced in volume by rotary evapn., saturated aq. soln. NH4PF6 added; mixt. cooled, ppt. filtered, dried, repttd. by ether from min. volume acetone, collected by filtration, chromed. on alumina column with toluene/acetonitrile mixt. as eluant, repptd. from CH2Cl2 by Et2O addn., filtered and dried; elem. anal.;

Reference yield:

cis-(Ru(bpy)2(p-CH2-cinn)2)(PF6)2 (85661-52-5) → (Ru(bpy)2(p-CH2-cinn)2)(PF6)2(polymer)

Guidance literature:

In acetonitrile; Electrochem. Process; electropolymerization complex in CH3CN-saturated nitrogen soln. by scanning Pt-disk potential repeatedly ca. 150 mV past E1/2 for the reductionwave of interest;

upstream raw materials:

N-(4-pyridylmethyl)cinnamamide

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